TPC-H2-Storage – Hydrogen storage

Infrastructure development for thermoplastic fiber composite pressure vessels for hydrogen storage and transport

With the project TPC-H2-STORAGE, IVW tapped into the growth potential of the hydrogen economy both technically and by expanding the institute's infrastructure, making it a central development partner and application centre for regional and national companies.

The research objective was to develop a new type of thermoplastic hydrogen pressure vessel. Figure 1 shows the final design of the tank and the production of the three preformed axial thermoplastic shells (0° fibre layers). The axially reinforced layers are produced using the 2D tape laying process and are then formed into a third shell. Circumferential layers were added by conventional winding process.

Significant investment has also been made in targeted testing and development of the materials used. This includes expanded process capabilities (e.g. laboratory hot press, industrial scale injection molding unit (Figure 2)), new testing equipment (e.g. cyclic tension-compression-torsion testing machine) and expanded analysis capabilities (e.g. broadband 2.5D scanning ultrasound system, Fourier transform infrared spectroscopy with thermal analysis).

In order to obtain a quality-assured component, all the data determined in the project was recorded and a digital twin of the tank was developed. This includes all aspects from the material to the finished component, leading to continuous application optimization throughout the life of the system.

The objective of the TPC-H2-STORAGE project is to establish a suitable infrastructure and fundamental knowledge to enable the future development of particularly efficient mobile as well as stationary hydrogen storage systems on a large scale using thermoplastic fiber composite structures.

Field of competence

Industry sectors

Project status

  • Current

M.Sc.

Christian Becker

Wiss. Mitarbeiter Bauweisen

Nanoscale Structure and Property Imaging by Cutting Edge AFM Techniques

Atomic force microscopy is a technique that has been used for over 30 years to characterize the surfaces of various solids. It is a scanning probe microscopy technique, in which the interaction of a very fine tip (tip radius down to 10 nm) and the surface of the sample to be examined is determined pixel by pixel. The tip sits at the end of a cantilever, which is deflected by attractive or repulsive interactions between the tip and the sample. This produces an image of the topography, with the resolution essentially determined by the radius of curvature of the tip.

With the AFM "Dimension IconIR" from Bruker, procured within the project "EFRE - REACT TPC-H2-Storage", it is now not only possible to image the topography of surfaces. In addition, by implementing novel AFM measurement modes, the following local material properties can also be mapped:

  • Peak Force QNM: characterization of nanomechanical properties (deformation, DMT modulus, pull-off force, dissipation).
  • Nano-DMA: nanoscale characterization of viscoelastic properties (storage modulus, loss modulus, loss factor)
  • AFM-IR: nanoscale resolution IR spectroscopy in the 1800-800 cm-1 wavenumber range.
  • Nano-TA: nanoscale thermal analysis in the range of RT - 350 °C.

With the AFM, it is now possible to study and correlate the morphology of composite materials and their properties on a microscopic scale at the same location on the sample. This makes it possible to draw correlations to macroscopic material properties and gain a comprehensive understanding of them. The information obtained will provide new approaches for the development of composites with (multi-)functional properties and their manufacturing processes.

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M.Sc.

Claudius Pirro

Scientific Staff Tailored Thermosets & Biomaterials

Funding

The project "TPC-H2-Storage - Infrastructure Development for Thermoplastic Fiber Composite Pressure Vessels for Hydrogen Storage and Transport" is funded by the European Regional Development Fund (ERDF) as part of the Union's response to the COVID-19 pandemic.